Researchers who often do experiments know that organic synthesis is a process of preparing more complex target molecules from simple raw materials through one or more chemical reactions. Generally, it requires fewer steps, and cheap raw materials. 24451-15-8, name is Ethyl 2-((4-bromophenyl)amino)-2-oxoacetate, A new synthetic method of this compound is introduced below., Computed Properties of C10H10BrNO3
General procedure: A methanolic solution of TBAOH (1.0 M, 2.4 mmol) was addeddirectly to a one-neck round flask suspension of the correspondingN-substituted oxamate proligand (0.6 mmol) in 10 mL of acetonitrileat 60 C. Then, an aqueous solution of K2[PdCl4] (100 mg,0.3 mmol in 5 mL of water) was added dropwise to the reactionmixture and resulting basic solution was heated at 60 C for 10 hunder continuous stirring. The solution was allowed to evaporateat room temperature. X-ray quality yellow prisms were grownup after two weeks (2) and a couple of days (3 and 4). Their formulaswere determined by X-ray diffraction on single crystals.2: Yield: 90%
The synthetic route of 24451-15-8 has been constantly updated, and we look forward to future research findings.
Reference:
Article; Fortea-Perez, Francisco Ramon; Neve, Francesco; Armentano, Donatella; De Munno, Giovanni; Stiriba, Salah-Eddine; Julve, Miguel; Inorganica Chimica Acta; vol. 443; (2016); p. 267 – 273;,
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