Category: 1118-92-9

Synthetic Route of 1118-92-9, The chemical industry reduces the impact on the environment during synthesis 1118-92-9, name is N,N-Dimethyloctanamide, I believe this compound will play a more active role in future production and life.

Example 2; 1-octanol was produced from N,N-dimethyloctanamide according to the following equation.[0084] [Chem. 13] [0085] 0.01 mmol of the complex 1 produced in Example 1 was placed in a 50 mL-autoclave equipped with a stirrer, and the autoclave was purged with nitrogen. 300 microliters of methanol, 1 mmol of N,N-dimethyloctanamide, and 500 microliters of methanol solution of 2.0 M sodium methoxide were added to the autoclave, and the autoclave was purged with hydrogen. The resulting mixture was stirred under hydrogen atmosphere (5 MPa) and 100 degrees C for 16 hours to obtain a reaction solution. The reaction solution was analyzed by gas chromatography, and as a result, it was confirmed that the GC area percentage of the amide as a raw material was 2% and the GC area percentage of 1-octanol was 92%.

In the field of chemistry, the synthetic routes of compounds are constantly being developed and updated. I will also mention this compound in other articles, N,N-Dimethyloctanamide, other downstream synthetic routes, hurry up and to see.

Reference:
Patent; TAKASAGO INTERNATIONAL CORPORATION; OGATA, Osamu; KURIYAMA, Wataru; MATSUMOTO, Takaji; WO2012/39098; (2012); A1;,
Amide – Wikipedia,
Amide – an overview | ScienceDirect Topics

1118-92-9, The chemical industry reduces the impact on the environment during synthesis 1118-92-9, name is N,N-Dimethyloctanamide, I believe this compound will play a more active role in future production and life.

In a 10 mL single-mouth bottle, nitrogen protection, adding 0.50 mmol of compound 1i,2.5 mL of n-hexane, 350 g/L aqueous sodium chloride solution (H2O: 1.0 mmol), 2.0 mmol of sodium dispersion reagent (34.1% by weight, suspension of mineral oil,Particle size <100mum), stirred at 0 C for 180min, raised to room temperature,The reaction was quenched with saturated aqueous sodium bicarbonate.Adding ether and saturated brine to extract, the organic phase is dried,Concentrated, separated by column chromatography,Obtained 29.3 mg of the target compound 3i,The yield was 37% The chemical industry reduces the impact on the environment during synthesis N,N-Dimethyloctanamide. I believe this compound will play a more active role in future production and life. Reference:
Patent; China Agricultural University; An Jie; Li Hengchao; Zhang Bin; Yan Yuhao; Luo Shihui; Zhang Yuntong; (23 pag.)CN110054538; (2019); A;,
Amide – Wikipedia,
Amide – an overview | ScienceDirect Topics