Synthetic Route of 101-21-3, In the next few decades, the world population will flourish. As the population grows rapidly and people all over the world use more and more resources, all industries must consider their environmental impact. 101-21-3, name is Isopropyl (3-chlorophenyl)carbamate belongs to amides-buliding-blocks compound, it is a common compound, a new synthetic route is introduced below.
A coprecipitation method was carried out to prepare the complex. beta-CD (2.270 g, 2.0 mmol) and CIPC (0.214 g, 1.0 mmol) were ground into powder together, then were completely dissolved in 100 mL of solution of ethanol and water (v/v = 1:5). The solution was stirred at 70C for 24 h, then ethanol was evaporated and the reaction mixture was cooled at 4C overnight. The precipitate was filtered and washed by a little doubly distilled water and ethanol,respectively. The obtained solid was dried to constant weight in a vacuum desiccator.
In the field of chemistry, the synthetic routes of compounds are constantly being developed and updated. I will also mention this compound in other articles, Isopropyl (3-chlorophenyl)carbamate, other downstream synthetic routes, hurry up and to see.
Reference:
Article; Ge, Xia; He, Jiang; Qi, Fengming; Yang, Ying; Huang, Zheng; Lu, Ruihua; Huang, Lizhen; Spectrochimica Acta Part A: Molecular and Biomolecular Spectroscopy; vol. 81; 1; (2011); p. 397 – 403;,
Amide – Wikipedia,
Amide – an overview | ScienceDirect Topics