Each compound has different characteristics, and only by selecting the characteristics of the compound suitable for a specific situation can the compound be applied on a large scale. 35303-76-5, name is 4-(2-Aminoethyl)benzenesulfonamide, This compound has unique chemical properties. The synthetic route is as follows., Safety of 4-(2-Aminoethyl)benzenesulfonamide
To a solution of 1- (3-isocyanatopropyl) -4-methoxybenzene (0.78 mmol) in THFWas added 4- (2-aminoethyl) benzenesulfonamide (0.86 mmol) at room temperature to a solution (20 ml)Was slowly added over 10-15 minutes. The reaction mixture was stirred at 40-45 [deg.] C for 24 hours. The next day TLC confirmed the termination of the reaction. The solvent was distilled off and ammonium chloride (100 & lt; RTI ID = 0.0 & gt;Ml), 1N HCl solution (50 ml) and ethyl acetate (100 ml). The organic layer was washed with brine and then dried with sodium sulfate. The solvent was distilled off and the residue was adsorbed onto silica gel using methylene chloride. The title compound was then purified by column chromatography using ethyl acetate and hexane.
According to the analysis of related databases, 35303-76-5, the application of this compound in the production field has become more and more popular.
Reference:
Patent; The Industry & Academic Cooperation in Chungnam National University (IAC); Jung, Sang-Hun; Woo, Sun-Hee; Kim, Sang- Kyum; Jeon, Eun-Seok; Lee, Yu-Jung; Meunikam, Manoj; Jalani, Hiteshkumar; Sharma, Niti; (205 pag.)KR2016/108281; (2016); A;,
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