Each compound has different characteristics, and only by selecting the characteristics of the compound suitable for a specific situation can the compound be applied on a large scale. 85006-25-3, name is tert-Butyl (tert-butoxycarbonyl)oxycarbamate, This compound has unique chemical properties. The synthetic route is as follows., Recommanded Product: 85006-25-3
Reagent and conditions: (a) tert-butyl (tert-butoxycarbonyl) oxycarbamate, 1N NaOH, TBAB, DCM; (b) TFA, DCM; (c) 2, 2-dimethylbutanoyl chloride, aq. NaHCO 3, THF, H 2O. Tert-butyl (tert-butoxycarbonyl) oxycarbamate (400 mg) and 1- (bromomethyl-d2) benzene-2, 3, 4, 5, 6-d5 (100mg) were dissolved in CH 2Cl 2 (4 ml) . The mixture was added 1M NaOH (2 ml) and tetrabutylammonium bromide (25.2 mg) , and stirred at room temperature for overnight. The resulting mixture was washed with water and dried with Na 2SO 4, concentrated in vacuo and purification by silica gel chromatography to give tert-butyl ( (tert-butoxycarbonyl) oxy) ( (phenyl- d5) methyl-d2) carbamate (510 mg, 99%) . 1HNMR (400 MHz, CDCl 3) delta 1.46 (s, 9H) , 1.44 (s, 9H) .
Chemical properties determine the actual use. Each compound has specific chemical properties and uses. We look forward to more synthetic routes in the future to expand reaction routes of 85006-25-3.
Reference:
Patent; SU, Yaning; SIRONAX LTD; ZHANG, Zhiyuan; YANG, Yi; WANG, Guozheng; LIU, Wendong; MA, Yongfen; REN, Yan; (74 pag.)WO2020/103859; (2020); A1;,
Amide – Wikipedia,
Amide – an overview | ScienceDirect Topics