Analyzing the synthesis route of 1-(Boc-amino)-3-butene

According to the analysis of related databases, 156731-40-7, the application of this compound in the production field has become more and more popular.

Each compound has different characteristics, and only by selecting the characteristics of the compound suitable for a specific situation can the compound be applied on a large scale. 156731-40-7, name is 1-(Boc-amino)-3-butene, This compound has unique chemical properties. The synthetic route is as follows., COA of Formula: C9H17NO2

3-chloro-perbenzoic acid (3 equiv) is added to an ice-cooled solution of t-butyl but-3-enyl- carbamate (1 equiv) in CH2CI2 in an inert atmosphere and stirred at 40 for 3 hours. The mixture obtained is cooled to 5 and quenched with saturated aq. sodium bisulfite solution. After extraction with CH2CI2, the combined organic layers obtained are washed 3 times with saturated aq. potassium carbonate solution, dried, filtered and concentrated.(+/-)-t-butyl (2-oxiranyl-ethyl)-carbamate is obtained.

According to the analysis of related databases, 156731-40-7, the application of this compound in the production field has become more and more popular.

Reference:
Patent; NOVARTIS AG; NOVARTIS PHARMA GMBH; WO2007/48771; (2007); A1;,
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