Synthetic Route of 104-10-9, As an important bridge between the micro and macro material world, chemistry is one of the main methods and means for humans to understand and transform the material world. 104-10-9, Name is 2-(4-Aminophenyl)ethanol, SMILES is NC1=CC=C(CCO)C=C1, belongs to amides-buliding-blocks compound. In a article, author is Roy, Sagar, introduce new discover of the category.
Simple Access to the Heaviest Alkaline Earth Metal Hydride: A Strongly Reducing Hydrocarbon-Soluble Barium Hydride Cluster
Reaction of Ba[N(SiMe3)(2)](2) with PhSiH3 in toluene gave simple access to the unique Ba hydride cluster Ba7H7[N-(SiMe3)(2)](7) that can be described as a square pyramid spanned by five Ba2+ ions with two flanking BaH[N(SiMe3)(2)] units. This heptanuclear cluster is well soluble in aromatic solvents, and the hydride (HNMR)-H-1 signals and coupling pattern suggests that the structure is stable in solution. At 95 degrees C, no coalescence of hydride signals is observed but the cluster slowly decomposes to undefined barium hydride species. The complex Ba7H7[N-(SiMe3)(2)](7) is a very strong reducing agent that already at room temperature reacts with Me3SiCH=CH2, norbornadiene, and ethylene. The highly reactive alkyl barium intermediates cannot be observed and deprotonate the (Me3Si)(2)N- ion, as confirmed by the crystal structure of Ba14H12[N(SiMe3)(2)](12)(-)[(Me3Si)(Me2SiCH2)N](4).
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