Joullie, Madeleine M. published the artcileReactions of amines with esters of polyhalogenated acids, Category: amides-buliding-blocks, the publication is Journal of the American Chemical Society (1955), 6662-3, database is CAplus.
Me2C:CH2 passed 1 hr. into 37 g. CF3CO2H (I) at 50°, and the mixture allowed to stand overnight, treated with more Me2C:CH2 until the heat evolution ceased, and fractionated yielded 75% CF3CO2CMe3 (II), b60 30°, b760 83°, nD25 1.3300. An appropriate ester treated gradually with the appropriate amine, and the mixture allowed to stand overnight and fractionated gave the corresponding amide; the mixtures with II were allowed to stand 4 days before fractionation. In this manner were prepared the following amides of I (m.p. or b.p./mm., % yield, nD25 given): di-Et, 30°/2, 60, 1.3780; piperidide, 44°/1, 84, 1.4153; morpholide, 47°/1, 87, 1.4177. C2F5CO2H: Bu, 48°/1, 80, 1.3642; morpholide, 59°/1 (m.p. 46-7°), 85, -. C3F7CO2H: Bu, 56°/2, 80, 1.3568; piperidide, 57°/2, 85, 1.3846; pyrrolidide, 65°/2, 76, 1.3755; morpholide, 72°/2, 89, 1.3850; piperidide of CHF2CO2H, 66°/3, 85, 1.4500. CClF2CO2H piperidide, 98°/10, 90, 1.4520. CHCl2CO2H pyrrolidide, 120°/2, 75, 1.5182.
Journal of the American Chemical Society published new progress about 360-92-9. 360-92-9 belongs to amides-buliding-blocks, auxiliary class Trifluoromethyl,Fluoride,Amine,Aliphatic hydrocarbon chain,Amide, name is N,N-Diethyl-2,2,2-trifluoroacetamide, and the molecular formula is C6H10F3NO, Category: amides-buliding-blocks.
Referemce:
https://en.wikipedia.org/wiki/Amide,
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