Fritz, H. published the artcileStudies on organophosphorus compounds. XXVI. Synthesis and carbon-13 NMR spectra of N,N-dialkyl thioamides, Category: amides-buliding-blocks, the publication is Bulletin des Societes Chimiques Belges (1978), 87(7), 525-34, database is CAplus.
By a new sulfuration reagent, the dimer of p-methoxyphenylthionophosphine sulfide, a series of thioamides were prepared in almost quant. yields from the corresponding amides. Carbon-13 NMR spectra of tertiary thioamides of formic, acetic, trifluoroacetic, propionic, and butyric acids were completely assigned with the aid of extensive double resonance and shift reagent experiments and the data obtained were compared with those of the analogous amides. A linear relation between the carbon-13 chem. shifts of the C:S of ethylthioamides and C:O of the corresponding amide was found.
Bulletin des Societes Chimiques Belges published new progress about 360-92-9. 360-92-9 belongs to amides-buliding-blocks, auxiliary class Trifluoromethyl,Fluoride,Amine,Aliphatic hydrocarbon chain,Amide, name is N,N-Diethyl-2,2,2-trifluoroacetamide, and the molecular formula is C6H10F3NO, Category: amides-buliding-blocks.
Referemce:
https://en.wikipedia.org/wiki/Amide,
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