Plakidin, V. L. et al. published their research in Zhurnal Organicheskoi Khimii in 1982 |CAS: 97-09-6

The Article related to substituted chlorobenzene amino nitrile, aniline derivative, benzenamine derivative, Benzene, Its Derivatives, and Condensed Benzenoid Compounds: Amines, Amine Oxides, Imines, and Quaternary Ammonium Compounds and other aspects.Synthetic Route of 97-09-6

On February 28, 1982, Plakidin, V. L.; Vostrova, V. N. published an article.Synthetic Route of 97-09-6 The title of the article was Reaction of 2,4-disubstituted chlorobenzenes with 3-alkylamino and 3-dialkylaminopropionitriles. And the article contained the following:

Reaction of I (R, R1 = H, NO2; NO2, NO2; NO2, Cl; NO2, SO2Me; NO2, SO2NH2; NO2, SO2NMe2; CN, NO2) with R22NCH2CH2CN (R2 = Me, Et) at 65-170° gave (via the quaternary salt) II (13 compounds), and with R2NHCH2CH2CN (R2 = Me, Et) at 20-130° gave III (11 compounds). At ∼130° cleavage of the cyanomethyl group from III was observed The experimental process involved the reaction of 3-Nitro-4-chlorobenzenesulfonamide(cas: 97-09-6).Synthetic Route of 97-09-6

The Article related to substituted chlorobenzene amino nitrile, aniline derivative, benzenamine derivative, Benzene, Its Derivatives, and Condensed Benzenoid Compounds: Amines, Amine Oxides, Imines, and Quaternary Ammonium Compounds and other aspects.Synthetic Route of 97-09-6

Referemce:
Amide – Wikipedia,
Amide – an overview | ScienceDirect Topics