Guillory, Paulette; Kapoor, Ramesh N.; Pannell, Keith H.; Schulte, Louis; McKee, Steven D.; Zhang, Zhi-Yi; Bartsch, Richard C. published the artcile< High yield, one-pot syntheses of symmetrical diaryl-N,N-dialkyl carbamoylmethylphosphine oxide (CMPO) ligands>, Electric Literature of 5326-82-9, the main research area is carbamoylmethylphosphine diaryl preparation; Grignard reagent coupling reaction phosphite chloroacetamide.
A simple 1-pot high yield (∼70%) process is reported for the synthesis, in ∼100 g amounts, of sym. diaryl-N,N-di-i-butylcarbamoylphosphine oxide (CMPO) actinide extractants, aryl = 4-t-butylphenyl, 4-trifluoromethylphenyl, 4-methoxyphenyl and 2,4,6-tri-i-propylphenyl.
Synthetic Communications published new progress about Coupling reaction. 5326-82-9 belongs to class amides-buliding-blocks, and the molecular formula is C10H20ClNO, Electric Literature of 5326-82-9.
Referemce:
Amide – Wikipedia,
Amide – an overview | ScienceDirect Topics