Gatrone, Ralph C.; Rickert, Paul G.; Horwitz, E. Philip; Smith, Barbara F.; Bartholdi, Catherine S.; Martinez, Aaron M. published the artcile< Analysis of n-octyl(phenyl)-N,N-diisobutylcarbamoylmethylphosphine oxide and TRUEX process solvent by gas and liquid chromatography>, Recommanded Product: 2-Chloro-N,N-diisobutylacetamide, the main research area is fuel reprocessing TRUEX solvent analysis chromatog; GC HPLC TRUEX solvent analysis; CMPO extractant analysis GC HPLC; octylphenyldiisobutylcarbamoylmethylphosphine oxide analysis GC HPLC; gas chromatog solvent analysis; liquid chromatog solvent analysis; phosphine oxide organic derivative analysis chromatog.
Complementary anal. procedures using capillary gas chromatog. (GC) and high-performance liquid chromatog. (HPLC) have been developed for the anal. of the TRUEX process solvents (CMPO-TBP-tetrachloroethylene or normal paraffinic hydrocarbons) and the extractant CMPO. GC analyses are accomplished in 20 min using a 15 m × 0.25 μm I.D. DB-5 capillary column with flame ionization detection. The anal. requires derivatization with diazomethane. HPLC analyses are performed in 10 min using a C18 reversed-phase column and a mobile phase consisting of acetonitrile-water-triethylamine (79:29.5:0.5) with refractive index and UV detection. The methods provide information regarding the presence of acidic and neutral impurities in stock extractant, fresh process solvent, and recovered TRUEX solvent.
Journal of Chromatography published new progress about Capillary gas chromatography. 5326-82-9 belongs to class amides-buliding-blocks, and the molecular formula is C10H20ClNO, Recommanded Product: 2-Chloro-N,N-diisobutylacetamide.
Referemce:
Amide – Wikipedia,
Amide – an overview | ScienceDirect Topics