Little discovery in the laboratory: a new route for 84547-64-8

《1,3- And 1,5-dimethylpyrazole-based syntheses. VI. Stilbene and 1,4-distyrylbenzene analogs containing 3-, 4-, and 5-pyrazolyl radicals》 provides a strategy for the preparation of materials with excellent comprehensive properties, which is conducive to broaden the application field of this compound(3-(Chloromethyl)-1-methyl-1H-pyrazole)Synthetic Route of C5H7ClN2.

Most of the natural products isolated at present are heterocyclic compounds, so heterocyclic compounds occupy an important position in the research of organic chemistry. A compound: 84547-64-8, is researched, SMILESS is CN1N=C(CCl)C=C1, Molecular C5H7ClN2Journal, Zhurnal Obshchei Khimii called 1,3- And 1,5-dimethylpyrazole-based syntheses. VI. Stilbene and 1,4-distyrylbenzene analogs containing 3-, 4-, and 5-pyrazolyl radicals, Author is Perevalov, V. P.; Karim, A. Kh.; Andreeva, M. A.; Rumyantseva, E. G.; Stepanov, B. I., the main research direction is pyrazolyl styrene IR fluorescence; aniline pyrazolylvinyl; nitrobenzene pyrazolylvinyl.Synthetic Route of C5H7ClN2.

Condensation of 4-O2NC6H4CH2CO2H with pyrazolecarboxaldehydes, followed by reduction with SnCl2, gave I (R, R1 = H, H; Me, H; H, Me). Appropriate Wittig reactions gave II (R = 1-methyl-3-pyrazolyl, 4,5-dichloro-1-methyl-3-pyrazolyl, 1-methyl-5-pyrazolyl, 4-chloro-1-methyl-5-pyrazolyl), which showed intensive blue fluorescence in PhMe solution

《1,3- And 1,5-dimethylpyrazole-based syntheses. VI. Stilbene and 1,4-distyrylbenzene analogs containing 3-, 4-, and 5-pyrazolyl radicals》 provides a strategy for the preparation of materials with excellent comprehensive properties, which is conducive to broaden the application field of this compound(3-(Chloromethyl)-1-methyl-1H-pyrazole)Synthetic Route of C5H7ClN2.

Reference:
Amide – Wikipedia,
Amide – an overview | ScienceDirect Topics