Application In Synthesis of Diphenylmethanamine. In 2020.0 CHEM SCI published article about ONE-POT SYNTHESIS; REDUCTIVE AMINATION; N-ALKYLATION; SELECTIVE SYNTHESIS; SECONDARY ALCOHOLS; AMMONIA; EFFICIENT; HYDROTALCITE; ADSORPTION; COMPLEXES in [Kita, Yusuke; Kuwabara, Midori; Yamadera, Satoshi; Kamata, Keigo; Hara, Michikazu] Tokyo Inst Technol, Lab Mat & Struct, Inst Innovat Res, Midori Ku, 4259 Nagatsuta Cho, Yokohama, Kanagawa 2268503, Japan; [Hara, Michikazu] Japan Sci & Technol Agcy JST, Adv Low Carbon Technol Res & Dev Program ALCA, 4-1-8 Honcho, Kawaguchi, Saitama 3320012, Japan in 2020.0, Cited 51.0. The Name is Diphenylmethanamine. Through research, I have a further understanding and discovery of 91-00-9.
Heterogeneously catalysed synthesis of primary amines by direct amination of alcohols with ammonia has long been an elusive goal. In contrast to reported Ru-based catalytic systems, we report that Ru-MgO/TiO(2)acts as an effective heterogeneous catalyst for the direct amination of a variety of alcohols to primary amines at low temperatures ofca.100 degrees C without the introduction of H(2)gas. The present system could be applied to a variety of alcohols and provides an efficient synthetic route for 2,5-bis(aminomethyl)furan (BAMF), an attention-getting biomonomer. The high catalytic performance can be rationalized by the reactivity tuning of Ru-H species using MgO. Spectroscopic measurements suggest that MgO enhances the reactivity of hydride species by electron donation from MgO to Ru.
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Reference:
Amide – Wikipedia,
,Amide – an overview | ScienceDirect Topics