Each compound has different characteristics, and only by selecting the characteristics of the compound suitable for a specific situation can the compound be applied on a large scale. 4141-08-6, name is 2-Amino-N-methylbenzamide, This compound has unique chemical properties. The synthetic route is as follows., Quality Control of 2-Amino-N-methylbenzamide
In a 250 mL reaction flask,A solution of 15 g (0.1 mol) of 2-amino-N-methylbenzamide,80 mL of acetonitrile was added,Ice bath temperature control below 10 ,33.75 g (0.25 mol) of sulfonyl chloride was slowly added dropwise,30min drops finished,Stirred at room temperature for 3 h,Most of the acetonitrile was distilled off under reduced pressure,With 20% Na2CO3 aqueous solution to adjust the pH to neutral,Filter,Washed,19.8 g of an off-white solid,Yield 90.4%.
Chemical properties determine the actual use. Each compound has specific chemical properties and uses. We look forward to more synthetic routes in the future to expand reaction routes of 4141-08-6.
Reference:
Patent; Qingdao University of Science and Technology; XU, LIANGZHONG; TIAN, SHUAIWANG; WANG, MINGHUI; (9 pag.)CN105153113; (2016); B;,
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