Researchers who often do experiments know that organic synthesis is a process of preparing more complex target molecules from simple raw materials through one or more chemical reactions. Generally, it requires fewer steps, and cheap raw materials. 83948-53-2, name is tert-Butyl N-(3-Bromopropyl)carbamate, A new synthetic method of this compound is introduced below., Product Details of 83948-53-2
Step 1 Preparation of Example 5a: (3-Methylamino-propyl)-carbamic Acid tert-butyl Ester Methylamine (100 mL of a 2.00 M solution in THF, 200 mmol) was added to (3-bromo-propyl)-carbamic acid tert-butyl ester (11.2 g, 47.0 mmol) at room temperature under nitrogen and the solution was stirred for 4 h. The resulting suspension was filtered and concentrated under reduced pressure to give 7.58 g (86%) of (3-methylamino-propyl)-carbamic acid tert-butyl ester (5a) as a clear oil. [M+H]+188.94.
The synthetic route of 83948-53-2 has been constantly updated, and we look forward to future research findings.
Reference:
Patent; KALYPSYS, INC.; US2007/123572; (2007); A1;,
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