Adding a certain compound to certain chemical reactions, such as: 685-91-6, name is N,N-Diethylacetamide, belongs to amides-buliding-blocks compound, can increase the reaction rate and produce products with better performance than those obtained under traditional synthetic methods. Here is a downstream synthesis route of the compound 685-91-6, HPLC of Formula: C6H13NO
General procedure: To the solution of 0.50 g (2.0 mmol) 2-bromo-3-aminobenzanthrone (1) in 2-3ml of appropriate amides, the phosphorusoxychloride (0.2 ml, 2.1 mmol) was added dropwise under stirring.The resulting mixture was heated for 3 h at 90-100 C. After cooling tothe ambient temperature, the crude product that precipitated onpouring into 50 ml of 2% NaOH water solution was filtered, washedwith water, and dried.
At the same time, in my other blogs, there are other synthetic methods of this type of compound, N,N-Diethylacetamide, and friends who are interested can also refer to it.
Reference:
Article; Kirilova; Puckins; Romanovska; Fleisher; Belyakov; Spectrochimica Acta Part A: Molecular and Biomolecular Spectroscopy; vol. 202; (2018); p. 41 – 49;,
Amide – Wikipedia,
Amide – an overview | ScienceDirect Topics