Synthetic Route of 2618-96-4, The chemical industry reduces the impact on the environment during synthesis 2618-96-4, name is Dibenzenesulfonimide, I believe this compound will play a more active role in future production and life.
Iodobenzene diacetate(579.8 mg, 1.8 mmol)And bis (benzenesulfonyl) imide(535.23 mg, 1.8 mmol) was added toIn acetonitrile,The mixture was stirred at 40 C. for 30 minutes.After that, N-pivaleindole (301.9 mg, 1.5 mmol) was added toAnd the mixture was stirred at room temperature for 3 hours.After removal of the solvent, ether was added,Filter,Washed with ethyl acetate,1- (2,2-Dimethyl-1-oxopropyl)-3- [bis(Benzenesulfone)Amidyl](Phenyl)-lambda 3 -iodanyl]-1 H-indole(893.28 mg, 85%).
In the field of chemistry, the synthetic routes of compounds are constantly being developed and updated. I will also mention this compound in other articles, Dibenzenesulfonimide, other downstream synthetic routes, hurry up and to see.
Reference:
Patent; Chiba University; Moriyama, Katsuhiko; Togo, Hideo; Ishida, Kazuma; (40 pag.)JP2015/34144; (2015); A;,
Amide – Wikipedia,
Amide – an overview | ScienceDirect Topics