In the chemical reaction process, reaction time, type of solvent, can easily affect the result of the reaction, thereby determining the yield and properties of the reaction product. An updated downstream synthesis route of 598-55-0 as follows. Product Details of 598-55-0
To a mixture of beta-naphthol (0.144 g, 1 mmol), arylaldehyde (1 mmol) and alkylcarbamate (1.3 mmol) in a test tube, was added nano-SB-[PSIM]Cl (0.01 g), and the resulting mixture was stirred magnetically at 70 C, and after solidification of the reaction mixture with a small rod at that temperature. The mixture was cooled to room temperature, then warm EtOAc (5 mL) was added and stirred for 1 min followed by centrifugation and decanting to separate nano-SB-[PSIM]Cl (the silica-bonded IL is not soluble in warm EtOAc, but the unreacted starting materials and the product are soluble in it). The separated EtOAc was evaporated, and the solid residue was recrystallized from hot EtOH (95 %) to give the pure alpha-carbamatoalkyl-beta-naphthol.
According to the analysis of related databases, 598-55-0, the application of this compound in the production field has become more and more popular.
Reference:
Article; Zare, Abdolkarim; Merajoddin, Maria; Moosavi-Zare, Ahmad Reza; Zarei, Mahmoud; Beyzavi, M. Hassan; Zolfigol, Mohammad Ali; Research on Chemical Intermediates; vol. 42; 3; (2016); p. 2365 – 2378;,
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