Reference of 63920-73-0, In the next few decades, the world population will flourish. As the population grows rapidly and people all over the world use more and more resources, all industries must consider their environmental impact. 63920-73-0, name is 2-Amino-4,6-dimethoxybenzamide belongs to amides-buliding-blocks compound, it is a common compound, a new synthetic route is introduced below.
Aniline 12 (37 mg, 0.188 mmol) and 14ba (47.0 mg, 0.188 mmol) weredissolved inDMAc (1.0 mL) and treated with sodium hydrogen sulfite (23.5mg,0.23 mmol) and PTSA (7.2 mg, 0.04 mmol). The reactionmixture was stirred at 120C for 16 h. Water was added to thereaction, and the precipitated solid wascollected by filtrationto give 15ba(69.0 mg, 86%).
In the field of chemistry, the synthetic routes of compounds are constantly being developed and updated. I will also mention this compound in other articles, 2-Amino-4,6-dimethoxybenzamide, other downstream synthetic routes, hurry up and to see.
Reference:
Article; Shao, Mingfeng; He, Linhong; Zheng, Li; Huang, Lingxiao; Zhou, Yuanyuan; Wang, Taijing; Chen, Yong; Shen, Mingsheng; Wang, Fang; Yang, Zhuang; Chen, Lijuan; Bioorganic and Medicinal Chemistry Letters; vol. 27; 17; (2017); p. 4051 – 4055;,
Amide – Wikipedia,
Amide – an overview | ScienceDirect Topics