In the next few decades, the world population will flourish. As the population grows rapidly and people all over the world use more and more resources, all industries must consider their environmental impact. 50487-72-4, name is N,N-Diallyl-4-methylbenzenesulfonamide belongs to amides-buliding-blocks compound, it is a common compound, a new synthetic route is introduced below. Quality Control of N,N-Diallyl-4-methylbenzenesulfonamide
General procedure: A solution of 18 (0.001-0.0025 mmol, 1.00 mol%-10.0 mol%) was added to a solution of alkene (0.10 mmol) in toluene (0.10 mL; 1.0 M) under nitrogen. The resulting mixture was stirred at 100 C for 2-12 h. Then, the solvent was removed under reduced pressure to yield a crude product, which was purified by flash chromatography (c-hexane-CH2Cl2) to remove the Ru residue. Conversions were obtained as confirmed by 1H NMR spectroscopy by comparing the ratios of the integrals of the starting materials with those of the products. The catalytic activities of ruthenium carbyne 18 to a variety of substrates are shown in Table 1.
The synthetic route of 50487-72-4 has been constantly updated, and we look forward to future research findings.
Reference:
Amide – Wikipedia,
Amide – an overview | ScienceDirect Topics