In the next few decades, the world population will flourish. As the population grows rapidly and people all over the world use more and more resources, all industries must consider their environmental impact. 758-96-3, name is N,N-Dimethylpropionamide belongs to amides-buliding-blocks compound, it is a common compound, a new synthetic route is introduced below. HPLC of Formula: C5H11NO
Weigh 6-methoxybenzothiazole (0.5mmol, 83mg), K2S2O8 (2mmol, 0.54g) and Eosin Y (0.01mmol, 6.5mg) in a 25mL Schlenk reaction tube, and then add N, N-dimethyl Propionamide (38mmol, 3.8g) was placed under a 20W power LED white light to react. The reaction was stirred at room temperature. The progress of the reaction was monitored by TLC. The reaction was completed after 24 hours. The reaction solution was concentrated to remove the solvent. Separation (eluent: petroleum ether / ethyl acetate with a volume ratio of 5: 1) gave a yellow oil, namely the derivative Il. Yield: 74%.
The synthetic route of 758-96-3 has been constantly updated, and we look forward to future research findings.
Reference:
Patent; Zhejiang University of Technology; Weng Jianquan; Xu Wenxiu; Dai Xiaoqiang; Liu Xinghai; (11 pag.)CN110432282; (2019); A;,
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