Reference of 5004-88-6, These common heterocyclic compound, 5004-88-6, name is 2-Amino-4,5-dimethoxybenzamide, its traditional synthetic route has been very mature, but the traditional synthetic route has various shortcomings, such as complicated route, low yield, poor purity, etc, below Introduce a new synthetic route.
To a stirred mixture of 4 g of 2-amino-4,5-dimethoxybenzamide and 200 ml of ether was added dropwise, e solution of 3.3 g of benzoyl isothiocyanate in 100 ml of ether over 15 minutes. After 24 hours, the solid was collected, giving 7 g of the desired product as white crystals, mp 204-207 C. (dec.).
Statistics shows that 2-Amino-4,5-dimethoxybenzamide is playing an increasingly important role. we look forward to future research findings about 5004-88-6.
Reference:
Patent; American Cyanamid Company; US5001157; (1991); A;,
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