In the next few decades, the world population will flourish. As the population grows rapidly and people all over the world use more and more resources, all industries must consider their environmental impact. 53844-02-3, name is Benzyl (2-bromoethyl)carbamate belongs to amides-buliding-blocks compound, it is a common compound, a new synthetic route is introduced below. Recommanded Product: 53844-02-3
Step 2 Synthesis of 3-(2-aminoethoxy)benzonitrile hydrobromide: 8 g of benzyl-N-(2-bromoethyl)carbamate, 3.7 g of 3-hydroxybenzonitrile, 4.3 g of calcium carbonate, 5.1 g of potassium iodide and 1.1 g of tetrabutylammonium iodide were stirred in dimethylformamide at 60C. After the treatment with ethyl acetate as the extractant in an ordinary manner, the product was purified by the silica gel column chromatography to obtain 3-[2-(benzyloxycarbonylamino)ethoxy]benzonitrile.
The synthetic route of 53844-02-3 has been constantly updated, and we look forward to future research findings.
Reference:
Patent; Ajinomoto Co., Inc.; EP976722; (2000); A1;,
Amide – Wikipedia,
Amide – an overview | ScienceDirect Topics