Adding a certain compound to certain chemical reactions, such as: 1118-69-0, name is N-Isopropylacetamide, belongs to amides-buliding-blocks compound, can increase the reaction rate and produce products with better performance than those obtained under traditional synthetic methods. Here is a downstream synthesis route of the compound 1118-69-0, 1118-69-0
Preparation of Zr(LMeJPr)4 (28). A 100 ml_ Schlenk flask, fitted with a reflux condenser, was charged with tetrakis(dimethylamido)zirconium (0.200 g, 0.748 mmol) and toluene (10 ml_). A solution of LMe iotaPrH (0.302 g, 2.99 mmol) in toluene (10 ml_) was added slowly and the resultant mixture was refluxed for 3 h. Upon cooling to room temperature, the volatile components were removed under reduced pressure and sublimation of the crude solid at 110 C/0.05 Torr afforded 28 as colorless crystals (0.188 g, 51 %): mp 206-209 0C.
In the field of chemistry, the synthetic routes of compounds are constantly being developed and updated. I will also mention this compound in other articles, N-Isopropylacetamide, other downstream synthetic routes, hurry up and to see.
Reference:
Patent; WAYNE STATE UNIVERSITY; WINTER, Charles, H.; KNISLEY, Thomas, Joseph; KARUNARATHNE, Panditha Koralalage, Don Mahesh Chinthaka; WO2010/132871; (2010); A1;,
Amide – Wikipedia,
Amide – an overview | ScienceDirect Topics