1118-92-9, The chemical industry reduces the impact on the environment during synthesis 1118-92-9, name is N,N-Dimethyloctanamide, I believe this compound will play a more active role in future production and life.
In a 10 mL single-mouth bottle, nitrogen protection, adding 0.50 mmol of compound 1i,2.5 mL of n-hexane, 350 g/L aqueous sodium chloride solution (H2O: 1.0 mmol), 2.0 mmol of sodium dispersion reagent (34.1% by weight, suspension of mineral oil,Particle size <100mum), stirred at 0 C for 180min, raised to room temperature,The reaction was quenched with saturated aqueous sodium bicarbonate.Adding ether and saturated brine to extract, the organic phase is dried,Concentrated, separated by column chromatography,Obtained 29.3 mg of the target compound 3i,The yield was 37%
The chemical industry reduces the impact on the environment during synthesis N,N-Dimethyloctanamide. I believe this compound will play a more active role in future production and life.
Reference:
Patent; China Agricultural University; An Jie; Li Hengchao; Zhang Bin; Yan Yuhao; Luo Shihui; Zhang Yuntong; (23 pag.)CN110054538; (2019); A;,
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