14433-76-2, In the chemical reaction process, reaction time, type of solvent, can easily affect the result of the reaction, thereby determining the yield and properties of the reaction product. An updated downstream synthesis route of 14433-76-2 as follows.
(0084) The hydrogenolysis of N,N-dimethyldecylamine works best with a 1:2 molar ratio of [Ru(triphos-(OMe)2)TMM] and B(C6F5)3. Thus, when N,N-dimethyldecylamine (1.0 mmol) was reacted at 160 C. under an atmosphere of H2 (100 bar) with [Ru(triphos-(OMe)2)TMM] (10 mumol) and 2 mol % B(C6F5)3, a conversion of 99% of the amide was observed. The reaction produced 3% decanol and 97% dimethyldecylamine.
At the same time, in my other blogs, there are other synthetic methods of this type of compound, 14433-76-2, and friends who are interested can also refer to it.
Reference:
Patent; Eastman Chemical Company; KLANKERMAYER, Juergen; WESTHUES, Stefan; LEITNER, Walter; HEMBRE, Robert Thomas; (11 pag.)US2019/345178; (2019); A1;,
Amide – Wikipedia,
Amide – an overview | ScienceDirect Topics